HCID 12237176、化合物 → HCID 14372148、化合物

HRID 1383000ノート

反応式

HRID 1383000 の反応式
[Cl:1][C:2]1[C:7]2[CH:8]=[CH:9][O:10][C:6]=2[CH:5]=[C:4](C)[N:3]=1.[CH3:12]C1C2OC=CC=2C(=O)NC=1.CC1NC(=O)C2C=COC=2C=1>>[Cl:1][C:2]1[C:7]2[CH:8]=[CH:9][O:10][C:6]=2[C:5]([CH3:12])=[CH:4][N:3]=1

参加物

4

反応物 3

HCID 12237176HCID 12237176、化合物HCID 122371844-chloro-6-methylfuro[3,2-c]pyridineHCID 14372147HCID 14372147、化合物

生成物 1

HCID 14372148HCID 14372148、化合物

実験手順

The title compound was prepared according to the procedure described for 4-chloro-6-methylfuro[3,2-c]pyridine (Example 12, Step B) except 7-methylfuro[3,2-c]pyridin-4-(5H)-one was substituted for 6-methylfuro[3,2-c]pyridin-4-(5H)-one. Title compound was obtained in 98% crude yield and used as is. A portion was crystallized from cold diethyl ether for microanalysis, mp. 51.5°-53° C.

後処理

  1. customThe title compound was prepared

出典と根拠

ORDレコード
ord-1c409d913b1d489db360b8fae7b353fe
出典データセット
uspto-grants-1989_02
特許番号
US04808595

反応ノート

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