関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-(2-Fluorocyclopentyloxy)-4-methoxybenzoic acid | HCID 21187946 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 3-(2-Fluorocyclopentyloxy)-4-methoxybenzoyl chloride | HCID 21187891 | — |
反応手順
A suspension of 3-(2-fluorocyclopentyloxy)-4-methoxybenzoic acid (0.48 g) in toluene (20 mL) is treated with thionyl chloride (0.34 g) and then is heated at 60° C. for 3 hours, and cooled and evaporated to give 3-(2-fluorocyclopentyl-oxy)-4-methoxybenzoyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06255326B1 |
|---|
| 出典データセット | uspto-grants-2001_07 |
|---|
| ORD ID | ord-546bbe33d58b4bef9e69285450de212d |
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| 出典メモ | uspto-grants-2001_07 |
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