化工社化工社 化学情報印刷レポート · 研究参考用
Nitric Acid → 6-Methyl-5-nitroquinoline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 6-Methylquinoline | HCID 7059 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | 6-Methyl-5-nitroquinoline | HCID 90009 | — |
反応手順
2.45 mol of 6-methylquinoline were added to 1 l of concentrated sulfuric acid, and 2.94 mol of 65% strength nitric acid were added dropwise at 0 to 10° C. The mixture was stirred for 1 hour, poured onto ice, adjusted to pH 2.5 with aqueous sodium hydroxide solution, filtered off with suction, washed with water and dried over magnesium sulfate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06262074B1 |
| 出典データセット | uspto-grants-2001_07 |
| ORD ID | ord-fa9a47705e954ea291f0c63fe138790b |
| 出典メモ | uspto-grants-2001_07 |