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Thionyl Chloride → 2-(4-ethoxyphenyl)acetyl Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | Benzeneacetic acid, 4-ethoxy- | HCID 78631 | — |
| 生成物 | 2-(4-ethoxyphenyl)acetyl Chloride | HCID 11629782 | — |
反応手順
50 g (0.28 mol) of 4-ethoxyphenylacetic acid were treated with 50 ml of thionyl chloride and the mixture was stirred for 24 hours at room temperature. Excess thionyl chloride was removed in vacuo and the residue was distilled under a high vacuum. This gave 39 g (71% of theory) of an oil (boiling point 110° C./53.3 Pa).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06265398B1 |
| 出典データセット | uspto-grants-2001_07 |
| ORD ID | ord-ab873478ff5c4224a1fffcfd1c5328c0 |
| 出典メモ | uspto-grants-2001_07 |