Hydrochloric Acid → HCID 23500354、化合物
反応式
[C:1]1([CH:9]=[C:7]([OH:8])[CH:6]=[C:4]([OH:5])[CH:3]=1)[OH:2].O=[C:11]1[CH2:16][CH2:15][CH:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:13][CH:12]1[C:23](OCC)=[O:24].Cl>C(O)C>[OH:2][C:1]1[C:9]2[C:11]3[CH2:16][CH2:15][CH:14]([C:17]4[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=4)[CH2:13][C:12]=3[C:23](=[O:24])[O:8][C:7]=2[CH:6]=[C:4]([OH:5])[CH:3]=1参加物
5
実験手順
A solution of phloroglucinol (1.56 g) and ethyl 2-oxo-5-phenylcyclohexane-carboxylate (2.52 g) in ethanol (25 ml) was treated with dry HCl as described in example 1a. The precipitate was filtered and washed with water and EtOH. Yield 1.0 g (32%).
後処理
- filtrationThe precipitate was filtered
- washwashed with water and EtOH
出典と根拠
- ORDレコード
- ord-d9d6656347494c5aab762fb43ff140c6
- 出典データセット
- uspto-grants-2001_07
- 特許番号
- US06265421B1
反応ノート
読み込み中…