化工社化工社 化学情報印刷レポート · 研究参考用
Tetrafluoroboric acid → Tricyclohexylphosphonium tetraphenylborate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tetrafluoroboric acid | HCID 28118 | — |
| 反応物 | Tricyclohexylphosphine | HCID 75806 | — |
| 反応物 | Sodium Tetraphenylborate | HCID 2723787 | — |
| 反応物 | Tricyclohexylphosphonium Tetrafluoroborate | HCID 11710396 | — |
| 生成物 | Tricyclohexylphosphonium tetraphenylborate | HCID 23136635 | 75% |
反応手順
Tricyclohexylphosphine is reacted with fluoroboric acid to synthesize tricyclohexylphosphonium tetrafluoroborate, which is reacted with sodium tetraphenylborate to produce tricyclohexylphosphonium tetraphenylborate (75% yield). A similar process is described in which tri-tert-butylphosphine is used as starting material to produce tri-tert-butylphosphonium tetraphenylborate (71% yield) (see Nonpatent Document 4).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07728176B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-26bcb57d0e5a476a8aaa17b3207a4354 |
| 出典メモ | uspto-grants-2010_06 |