化工社化工社 化学情報印刷レポート · 研究参考用
(4-Methoxyphenyl)boronic acid → 2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4-Methoxyphenyl)boronic acid | HCID 201262 | — |
| 反応物 | 2-Iodo-3-(4-methoxyphenoxy)benzo[b]thiophene | HCID 10691279 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene | HCID 11793004 | 70% |
反応手順
By essentially following the procedure detailed in Example 1, Part B, the title compound was prepared from 2-iodo-3-(4-methoxyphenoxy)benzo[b]thiophene (Part B) and (4-methoxyphenyl)boronic acid (Part C) in 70% yield following chromatography (SiO2; 5% EtOAc in hexanes).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06265575B1 |
| 出典データセット | uspto-grants-2001_07 |
| ORD ID | ord-c0ce58324bd54ddb9494a30ba4e3b937 |
| 出典メモ | uspto-grants-2001_07 |