2-(4-Methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene → 4-[[2-(4-Hydroxyphenyl)benzo[b]thiophen-3-yl]oxy]phenol
反応式
C[O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[S:13][C:12]3[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=3[C:10]=2[O:18][C:19]2[CH:24]=[CH:23][C:22]([O:25]C)=[CH:21][CH:20]=2)=[CH:5][CH:4]=1>CCOC(C)=O>[OH:2][C:3]1[CH:4]=[CH:5][C:6]([C:9]2[S:13][C:12]3[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=3[C:10]=2[O:18][C:19]2[CH:20]=[CH:21][C:22]([OH:25])=[CH:23][CH:24]=2)=[CH:7][CH:8]=1参加物
3
実験手順
By essentially following the procedure detailed in Example 5, Part B, the title compound was prepared from 2-(4-methoxyphenyl)-3-(4-methoxyphenoxy)benzo[b]thiophene (Part D) in 87% yield following radial chromatography (SiO2; 25% EtOAc in hexanes).
出典と根拠
- ORDレコード
- ord-8be568f2b5414df185cfc1bcc1805223
- 出典データセット
- uspto-grants-2001_07
- 特許番号
- US06265575B1
反応ノート
読み込み中…