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HRID 1389520作成日:2026年10月27日

Benzene → 4-Vinylpyridine styrene

https://huagongshe.com/reaction/1389520

反応式

関与物質

役割名称HCID仕込み量
反応物BenzeneHCID 241—
反応物AzobisisobutyronitrileHCID 6547—
反応物StyreneHCID 7501—
反応物2-VinylpyridineHCID 7521—
溶媒HexaneHCID 8058—
生成物4-Vinylpyridine styreneHCID 1266645520%

反応手順

In a 200 ml three necked flask were charged 21 g of 4-vinylpyridine, 21 g of styrene and 0.1 g of azobisisobutyronitrile and 90 ml of benzene. The mixture was polymerized at 80° C. for 6 hrs under a nitrogen atmosphere. The reaction liquid was poured into a large amount of n-hexane to thereby obtain white precipitates. After filtering and drying, a white powder was obtained. The molar fraction of vinylpyridine in the polymer was 0.57 and the yield was 20%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04245027
出典データセットuspto-grants-1981_01
ORD IDord-2fc78f28946d42f0a1e6089859ad9551
出典メモuspto-grants-1981_01