Naphthalene → 1-Naphthalenesulfonic acid
反応式
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[S:11](=O)(=[O:14])([OH:13])[OH:12]>>[C:9]1([S:11]([OH:14])(=[O:13])=[O:12])[C:10]2[C:5](=[CH:4][CH:3]=[CH:2][CH:1]=2)[CH:6]=[CH:7][CH:8]=1参加物
3
反応条件
- 温度
- 150 °C
実験手順
256 g naphthalene (2.0 m) and 200 g sulfuric acid 98% (2.0 m) were charged to a reactor and mixed. The mixture was then heated rapidly to 150° C. and agitated at 150° C. for 2 hours. Then 100 g sulfuric acid 98% was added and the mixture agitated for an additional hour to obtain the naphthalenesulfonic acid.
後処理
- additionmixed
- stirringthe mixture agitated for an additional hour
出典と根拠
- ORDレコード
- ord-cbc305bac623410f9a0bb501d6d51c03
- 出典データセット
- uspto-grants-1981_01
- 特許番号
- US04245994
反応ノート
読み込み中…