1,10-Decanediamine → N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine]

HRID 1391144ノート

反応式

HRID 1391144 の反応式
[CH2:1]1[O:7][CH:2]1[CH2:3][CH2:4][CH2:5][CH3:6].[CH2:8]([NH2:19])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][NH2:18]>C(O)(C)C>[CH2:17]([NH:18][CH2:1][CH:2]([OH:7])[CH2:3][CH2:4][CH2:5][CH3:6])[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][NH:19][CH2:1][CH:2]([OH:7])[CH2:3][CH2:4][CH2:5][CH3:6]

参加物

4

反応物 2

HCID 13171,10-DecanediamineHCID 150362-Butyloxirane

生成物 1

HCID 21332454N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine]

試薬・触媒・溶媒 1

HCID 3776Isopropanol溶媒

実験手順

In a manner similar to that of Example 1, condensation of 1-hexene oxide (34.8 g.) and 1,10-decanediamine (30 g.) and recrystallization of the resulting product from isopropyl alcohol gave N,N'-(1,10-decylene)-bis[2-hydroxyhexylamine] (I: R = CH3 (CH2)3, R' = H, X = (CH2)10, Z = H) (8.9 g., m.p. 127.0°-137.0° C.).

出典と根拠

ORDレコード
ord-7bd6cd34deff418bae8148468a0f6028
出典データセット
uspto-grants-1979_02
特許番号
US04140860

反応ノート

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