化工社化工社 化学情報印刷レポート · 研究参考用
4,4-Bis(methoxymethyl)biphenyl → [1,1'-Biphenyl]-4,4'-dicarboxaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4,4-Bis(methoxymethyl)biphenyl | HCID 1519430 | — |
| 反応物 | Sodium Bromate | HCID 23668195 | — |
| 生成物 | [1,1'-Biphenyl]-4,4'-dicarboxaldehyde | HCID 6200 | — |
反応手順
In the same manner as in Example 3, the operation was conducted, except that 0.53 g (2 mmols) of bismethoxymethylbiphenyl was used in place of m-methoxybenzyl alcohol and also 0.2 g (1.35 mmols) of sodium bromate was used. With respect to the components in the reaction solution, 4,4′-bisformylbiphenyl was produced in an area ratio, as determined by gas chromatography, of 93.3% and 6.7% of bismethoxymethylbiphenyl as a raw material was remained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07342138B2 |
| 出典データセット | uspto-grants-2008_03 |
| ORD ID | ord-5860edf70f8347c2b5e0d67f6c44c247 |
| 出典メモ | uspto-grants-2008_03 |