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HRID 1392571作成日:2026年10月27日

4,4-Bis(methoxymethyl)biphenyl → [1,1'-Biphenyl]-4,4'-dicarboxaldehyde

https://huagongshe.com/reaction/1392571

反応式

関与物質

役割名称HCID仕込み量
反応物4,4-Bis(methoxymethyl)biphenylHCID 1519430—
反応物Sodium BromateHCID 23668195—
生成物[1,1'-Biphenyl]-4,4'-dicarboxaldehydeHCID 6200—

反応手順

In the same manner as in Example 3, the operation was conducted, except that 0.53 g (2 mmols) of bismethoxymethylbiphenyl was used in place of m-methoxybenzyl alcohol and also 0.2 g (1.35 mmols) of sodium bromate was used. With respect to the components in the reaction solution, 4,4′-bisformylbiphenyl was produced in an area ratio, as determined by gas chromatography, of 93.3% and 6.7% of bismethoxymethylbiphenyl as a raw material was remained.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07342138B2
出典データセットuspto-grants-2008_03
ORD IDord-5860edf70f8347c2b5e0d67f6c44c247
出典メモuspto-grants-2008_03