Hydrochloric Acid → HCID 69203826、化合物

HRID 1393057ノート

反応式

HRID 1393057 の反応式
[CH3:1][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([O:10]C)=[O:9])[CH3:3].[ClH:18]>>[ClH:18].[CH3:3][N:2]([CH2:4][C:5]1[C:6]([N+:15]([O-:17])=[O:16])=[C:7]([CH:12]=[CH:13][CH:14]=1)[C:8]([OH:10])=[O:9])[CH3:1]

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 23144875HCID 23144875、化合物

生成物 1

HCID 69203826HCID 69203826、化合物

反応条件

温度
100 °C

実験手順

The mixture of methyl 3-dimethylaminomethyl-2-nitrobenzoate (0.72 g) and 6M hydrochloric acid was stirred at 100° C. overnight. After cooling the mixture to room temperature, the precipitated crystals were filtered out, washed with diethylether and dried under reduced pressure to obtain 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride.

後処理

  1. temperatureAfter cooling the mixture to room temperature
  2. filtrationthe precipitated crystals were filtered out
  3. washwashed with diethylether
  4. customdried under reduced pressure

出典と根拠

ORDレコード
ord-86c0a1d8138449b88f5963e6dbc7ac35
出典データセット
uspto-grants-2008_03
特許番号
US07345049B2

反応ノート

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