Aniline → 2-Butylmercaptoaniline

HRID 1395108

反応式

HRID 1395108 の反応式
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[SH:10])([O-])=O.N[C:12]1[CH:17]=CC=[CH:14][CH:13]=1.C(N1CCCC1=O)O>>[CH2:17]([S:10][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[NH2:1])[CH2:12][CH2:13][CH3:14]

参加物

4

実験手順

2-Butylmercaptoaniline was prepared from -2-nitrothiophenol by a two-step reaction sequence consisting of alkylation followed by reduction corresponding to the procedure described in Example 4. The aniline then was condensed with N-methylol-2-pyrrolidone to yield the desired product.

後処理

  1. customby a two-step reaction sequence

出典と根拠

ORDレコード
ord-1896fe5c8dbc4c8cb91fe8c65ef0af82
出典データセット
uspto-grants-1980_05
特許番号
US04202821

関連ノート

読み込み中…