Ethylenediamine → HCID 86633218、化合物

HRID 1395973ノート

反応式

HRID 1395973 の反応式
[C:1]1([S:7](OCCCCCCCCCCCC)(=O)=O)C=CC=CC=1.[Na].[CH2:24]([NH2:27])[CH2:25]N.[O:28]=[N+:29]([O-:34])[C:30]([Cl:33])([Cl:32])[Cl:31]>O.C(N=C=S)C=C>[CH2:24]([N:27]=[C:1]=[S:7])[CH:25]=[CH2:30].[O:28]=[N+:29]([O-:34])[C:30]([Cl:33])([Cl:32])[Cl:31]

参加物

6

反応物 3

HCID 3301EthylenediamineHCID 6423ChloropicrinHCID 57371080Sodium dodecylbenzene sulphonate

生成物 1

HCID 86633218HCID 86633218、化合物

試薬・触媒・溶媒 2

HCID 962Water溶媒2 回HCID 5971Allyl Isothiocyanate溶媒

実験手順

The aqueous phase is prepared by dissolving 1.0 g of sodium dodecyl benzenesulphonate in 100 ml of water. The organic phase is prepared by dissolving 3.0 g of poly[(phenyl isocyanate)-co-formaldehyde] (Mn about 400) in a mixture of 5 g of allyl isothiocyanate and 15 g of chloropicrin. The two phases are emulsified with a rod mixer at a rate of about 350 r.p.m. for 3 minutes at room temperature. During the emulsification an aqueous solution is added, obtained by diluting 0.70 g of ethylenediamine in 30 ml of water. The reaction is carried out for about three hours. At the end of the reaction, the preparation is preserved as such ready for use.

後処理

  1. customThe aqueous phase is prepared
  2. customThe organic phase is prepared
  3. additionDuring the emulsification an aqueous solution is added
  4. customobtained
  5. waitThe reaction is carried out for about three hours
  6. customAt the end of the reaction

出典と根拠

ORDレコード
ord-ce0ea8e1b84a4225a56b3e36de0fb41e
出典データセット
uspto-grants-2014_12
特許番号
US08901037B2

反応ノート

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