反応式
C(OC([N:8]1[CH2:14][CH2:13][CH2:12][N:11]([C:15](=[S:17])[NH2:16])[CH2:10][CH2:9]1)=O)(C)(C)C.Br[CH2:19][C:20]([C:22]1[CH:31]=[CH:30][C:29]2[C:28]([CH3:33])([CH3:32])[CH2:27][CH2:26][C:25]([CH3:35])([CH3:34])[C:24]=2[CH:23]=1)=O>>[CH3:32][C:28]1([CH3:33])[CH2:27][CH2:26][C:25]([CH3:34])([CH3:35])[C:24]2[CH:23]=[C:22]([C:20]3[N:16]=[C:15]([N:11]4[CH2:12][CH2:13][CH2:14][NH:8][CH2:9][CH2:10]4)[S:17][CH:19]=3)[CH:31]=[CH:30][C:29]1=2参加物
3
実験手順
The preparation is carried out as already described starting from 1.12 g (4.55 mmol) of 4-thiocarbamoyl-1,4-diazepane-1-carboxylic acid tert-butyl ester from step a and 1.93 g (6.25 mmol) of 2-bromo-1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)ethanone.
出典と根拠
- ORDレコード
- ord-afa24e65d6414065ab068d5c42c7e3ee
- 出典データセット
- uspto-grants-2014_12
- 特許番号
- US08907098B2
関連ノート
読み込み中…