4-Chlorobenzaldehyde → 3-(4-Chlorophenyl)-1-(4-ethylphenyl)prop-2-en-1-one

反応式

[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.[CH3:10][CH2:11][C:12]1[CH:17]=[CH:16][C:15]([C:18]([CH3:20])=[O:19])=[CH:14][CH:13]=1>>[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[CH:20][C:18]([C:15]2[CH:16]=[CH:17][C:12]([CH2:11][CH3:10])=[CH:13][CH:14]=2)=[O:19])=[CH:4][CH:3]=1

参加物

反応物 2

HCID 77264-Chlorobenzaldehyde

HCID 136424'-Ethylacetophenone

生成物 1

HCID 41009983-(4-Chlorophenyl)-1-(4-ethylphenyl)prop-2-en-1-one

実験手順

By a procedure similar to that of example 1.59.1, starting from 4-chlorobenzaldehyde and 4-ethylacetophenone, 3-(4-chlorophenyl)-1-(4-ethylphenyl)prop-2-en-1-one was obtained as pale yellowish solid.

出典と根拠

ORDレコード: ord-fa57978a11554088af8f1c44543811a3
出典データセット: uspto-grants-2014_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08912186B2

反応ノート

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