HCID 21491380、化合物 → HCID 59467883、化合物
反応式
Cl[CH2:2][C:3]([N:5]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][C:13]=2[CH3:15])[CH2:8][CH2:7][CH2:6]1)=[O:4].[Cl:16][C:17]1[CH:18]=[CH:19][C:20]2[S:24][C:23]([SH:25])=[N:22][C:21]=2[CH:26]=1>>[Cl:16][C:17]1[CH:18]=[CH:19][C:20]2[S:24][C:23]([S:25][CH2:2][C:3]([N:5]3[C:14]4[C:9](=[CH:10][CH:11]=[CH:12][C:13]=4[CH3:15])[CH2:8][CH2:7][CH2:6]3)=[O:4])=[N:22][C:21]=2[CH:26]=1参加物
3
実験手順
The title compound was synthesized according to General Procedure A using compound 2 as the electrophile and 5-chloro-2-mercaptobenzothiazole as the nucleophile to yield 15 (3.60 g, 56%): MS m/z: 393 (M+H)+. Anal. Calcd. For, C19H17ClN2OS2.0.2H2O: C, 58.14; H, 4.47; N, 7.14; S, 16.33; Cl, 9.03. Found: C, 57.90; H, 4.40; N, 7.17; S, 16.47; Cl, 9.24.
後処理
- customThe title compound was synthesized
出典と根拠
- ORDレコード
- ord-5482eed4f3e546cebbdcfaeb367d0851
- 出典データセット
- uspto-grants-2014_12
- DOI