化工社化工社 化学情報印刷レポート · 研究参考用
3-Methoxybenzenethiol → {[4-Hydroxy-1-(3-methoxy-phenylsulfanyl)-isoquinoline-3-carbonyl]-amino}-acetic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methoxybenzenethiol | HCID 84989 | — |
| 反応物 | FG-2216 | HCID 6914666 | — |
| 生成物 | {[4-Hydroxy-1-(3-methoxy-phenylsulfanyl)-isoquinoline-3-carbonyl]-amino}-acetic acid | HCID 66712952 | — |
反応手順
The title compound was prepared from [(1-chloro-4-hydroxy-isoquinoline-3-carbonyl)-amino]-acetic acid (U.S. Pat. No. 6,093,730) and 3-methoxybenzenethiol under conditions analogous to Example D-110. The final product was precipitated from a solution of ethyl acetate using hexanes; MS (−) m/z 385.12 (M−1)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08916585B2 |
| 出典データセット | uspto-grants-2014_12 |
| ORD ID | ord-ab1c8e436ab44863bcd4ac3822915992 |
| 出典メモ | uspto-grants-2014_12 |