1-Bromo-3,5-difluorobenzene → 3,5-Difluoro-4'-methoxybenzophenone
反応式
Br[C:2]1[CH:7]=[C:6]([F:8])[CH:5]=[C:4]([F:9])[CH:3]=1.[CH3:10][O:11][C:12]1[CH:22]=[CH:21][C:15]([C:16](C(Cl)=O)=[O:17])=[CH:14][CH:13]=1>>[F:9][C:4]1[CH:3]=[C:2]([CH:7]=[C:6]([F:8])[CH:5]=1)[C:16]([C:15]1[CH:21]=[CH:22][C:12]([O:11][CH3:10])=[CH:13][CH:14]=1)=[O:17]参加物
3
実験手順
The procedure from Step 1 of Example 1 was followed except that: 1-bromo-3,5-difluorobenzene was used instead of tribromobenzene and 4-methoxybenzoyl carbonyl chloride was used in place of benzoyl chloride to provide a product with mass spectrum corresponding the structure of 3,5-difluoro-4′-methoxybenzophenone.
出典と根拠
- ORDレコード
- ord-951c0fb5c8304d60bfb8c32fc4ab6c9a
- 出典データセット
- uspto-grants-2014_12
- 特許番号
- US08920928B2
反応ノート
読み込み中…