2-(Dimethylamino)ethanol → 2-(Dimethylamino)ethanol

HRID 1414152

反応式

HRID 1414152 の反応式
[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][OH:5].C([CH:19]1[CH2:24][C:23](=[O:25])[O:22][C:20]1=[O:21])CCCCCCCCCCC>O=C1CC(C)(C)CC(C)=C1>[CH3:1][N:2]([CH3:6])[CH2:3][CH2:4][OH:5].[C:20]1(=[O:21])[O:22][C:23](=[O:25])[CH:24]=[CH:19]1

参加物

5

反応物 2

HCID 79022-(Dimethylamino)ethanolHCID 98107Dodecylsuccinic anhydride

生成物 2

HCID 79022-(Dimethylamino)ethanolHCID 7923Maleic Anhydride

試薬・触媒・溶媒 1

HCID 6544Isophorone溶媒

反応条件

温度
70 °C

実験手順

A reaction vessel containing 53.5 parts of Polyepoxide A (80 percent solids in isophorone) was heated to 70°C. There were added 3 parts of an amine produced by reacting dimethylethanolamine with dodecylsuccinic anhydride, and then there were added 6 parts of a second amine produced from dimethylethanolamine and maleic anhydride. During the second addition the temperature was raised to 95°C. and stirring was continued for 15 minutes at this temperature. The product when diluted with water and electrodeposited, as in the above examples, provided an adherent solvent-resistant coating.

後処理

  1. customproduced

出典と根拠

ORDレコード
ord-664b2dbd034848599956c811643f942d
出典データセット
uspto-grants-1977_01
特許番号
US04001101

関連ノート

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