Benzylamine → HCID 21487297、化合物
反応式
O1C=CC=C1C[NH:7][C:8]1[C:9](=[CH:13][C:14]([S:25](=[O:28])(=[O:27])[NH2:26])=[C:15]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([Cl:24])[CH:19]=2)[CH:16]=1)[C:10]([OH:12])=[O:11].[CH2:29]([NH2:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[CH2:29]([NH:36][NH:7][C:8]1[C:9](=[CH:13][C:14]([S:25](=[O:27])(=[O:28])[NH2:26])=[C:15]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([Cl:24])[CH:19]=2)[CH:16]=1)[C:10]([OH:12])=[O:11])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1参加物
3
実験手順
45.5 g of the carboxylic acid prepared in Example 9 (b) (0.1 mol) were reacted with 100 ml of benzylamine as in Example 9 (c), and the reaction product was purified by recrystallization from ethanol.
後処理
- customthe reaction product was purified by recrystallization from ethanol
出典と根拠
- ORDレコード
- ord-26bc100085c34a1981b3bb28f0faec69
- 出典データセット
- uspto-grants-1977_01
- 特許番号
- US04001284