2,3-Dihydro-1-benzofuran-6-ol → 6-[(3,7-Dimethylnona-2,6-dien-1-YL)oxy]-2,3-dihydro-1-benzofuran

反応式

Br[CH2:2][CH:3]=[C:4]([CH3:12])[CH2:5][CH2:6][CH:7]=[C:8]([CH3:11])[CH2:9][CH3:10].[OH:13][C:14]1[CH:22]=[CH:21][C:17]2[CH2:18][CH2:19][O:20][C:16]=2[CH:15]=1>>[CH3:12][C:4]([CH2:5][CH2:6][CH:7]=[C:8]([CH3:11])[CH2:9][CH3:10])=[CH:3][CH2:2][O:13][C:14]1[CH:22]=[CH:21][C:17]2[CH2:18][CH2:19][O:20][C:16]=2[CH:15]=1

参加物

反応物 2

HCID 122365402,3-Dihydro-1-benzofuran-6-ol

HCID 536807021-Bromo-3,7-dimethyl-2,6-nonadiene

生成物 1

HCID 536330946-[(3,7-Dimethylnona-2,6-dien-1-YL)oxy]-2,3-dihydro-1-benzofuran

実験手順

1-bromo-3,7-dimethyl-2,6-nonadiene and 6-hydroxy-2,3-dihydrobenzofuran are reacted to form 6-[(3,7-dimethyl-2,6-nonadienyl)-oxy]-2,3-dihydrobenzofuran of boiling point 138° C./0.002 mmHg; nD20 = 1.5382;

出典と根拠

ORDレコード: ord-9f1e97cfaf98441f8a6f76b6cfe21603
出典データセット: uspto-grants-1977_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04002647

反応ノート

読み込み中…