化工社化工社 化学情報印刷レポート · 研究参考用
Trimethylsilyl cyanide → alpha-(4-Chlorophenyl)-alpha-(4-methylthioanilino)acetonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trimethylsilyl cyanide | HCID 82115 | — |
| 反応物 | N-(4-Chlorobenzylidene)-4-methylthioaniline | HCID 21862850 | — |
| 生成物 | alpha-(4-Chlorophenyl)-alpha-(4-methylthioanilino)acetonitrile | HCID 21862778 | — |
反応手順
Following a procedure similar to that described in Example 1(ii), but using N-(4-chlorobenzylidene)-4-methylthioaniline [prepared as described in step (i) above] and trimethylsilyl cyanide as starting materials, the title compound was obtained as a pale yellow powder (yield 84%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05908858 |
| 出典データセット | uspto-grants-1999_06 |
| ORD ID | ord-2e9f2f90c0854982aeddef6faa5ef0ca |
| 出典メモ | uspto-grants-1999_06 |