p-Toluidine → N-(4-Sulfamoylbenzylidene)-4-methylaniline

反応式

[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=O)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2].[CH3:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][CH:15]=1>>[S:1]([C:5]1[CH:12]=[CH:11][C:8]([CH:9]=[N:18][C:17]2[CH:19]=[CH:20][C:14]([CH3:13])=[CH:15][CH:16]=2)=[CH:7][CH:6]=1)(=[O:4])(=[O:3])[NH2:2]

参加物

反応物 2

HCID 7813p-Toluidine

HCID 1510884-Sulfamoylbenzaldehyde

生成物 1

HCID 21862824N-(4-Sulfamoylbenzylidene)-4-methylaniline

実験手順

Following a procedure similar to that described in Example 1(i), but using 4-sulfamoylbenzaldehyde and 4-methylaniline as starting materials, the title compound was obtained as a yellow powder (yield 82%).

出典と根拠

ORDレコード: ord-ccc50503d20a417d92b2494d77b95924
出典データセット: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05908858

反応ノート

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