Benzaldehyde → 4-(Benzylideneamino)benzenesulfonamide

反応式

[CH:1](=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[S:9]([C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][CH:14]=1)(=[O:12])(=[O:11])[NH2:10]>>[CH:1](=[N:17][C:16]1[CH:18]=[CH:19][C:13]([S:9](=[O:12])(=[O:11])[NH2:10])=[CH:14][CH:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

反応物 2

HCID 240Benzaldehyde

HCID 5333Sulfanilamide

生成物 1

HCID 3084054-(Benzylideneamino)benzenesulfonamide

実験手順

Following a procedure similar to that described in Example 1(i), but using benzaldehyde and 4-sulfamoylaniline as starting materials, the title compound was obtained as a pale yellow powder (yield 91%).

出典と根拠

ORDレコード: ord-692ffe7121b44d158d73d633c53c3db2
出典データセット: uspto-grants-1999_06
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05908858

反応ノート

読み込み中…