化工社化工社 化学情報印刷レポート · 研究参考用
Triolein → Tristearin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triolein | HCID 5497163 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | Tristearin | HCID 11146 | 23% |
反応手順
In a second hexane fractionation, above olein-fraction was fractionated, (3,22:1 hexane to oil ratio at -10° C.); a stearin fraction was obtained. This stearin fraction contained 60 wt % of diglycerides of which 56,7 wt % were of the SU-type. The overall yield from fractionations was 29%. A third fractionation was performed on the stearin fraction obtained (5:1 hexane to oil at 24,5° C.). The olein-fraction was collected, it contained 62 wt % of diglycerides of which 72,5 wt % were SU-diglycerides. The overall yield was 23%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05912042 |
| 出典データセット | uspto-grants-1999_06 |
| ORD ID | ord-89cfdcf4d66944ccbf7cfbfc5b18ae82 |
| 出典メモ | uspto-grants-1999_06 |