Hydrochloric Acid → 8-Amino-octanoic acid methyl-butyl-amide hydrochloric acid salt

HRID 1417421ノート

反応式

HRID 1417421 の反応式
[CH3:1][N:2]([CH2:20][CH2:21][CH2:22][CH3:23])[C:3](=[O:19])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][NH:11]C(OC(C)(C)C)=O.[ClH:24]>O1CCOCC1>[ClH:24].[CH3:1][N:2]([CH2:20][CH2:21][CH2:22][CH3:23])[C:3](=[O:19])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][NH2:11]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 537219698-(t-Butoxycarbonyl)amino-octanoic acid methyl-butyl-amide

生成物 1

HCID 867537598-Amino-octanoic acid methyl-butyl-amide hydrochloric acid salt

試薬・触媒・溶媒 1

HCID 312751,4-Dioxane溶媒

実験手順

Combine 8-(t-butoxycarbonyl)amino-octanoic acid methyl-butyl-amide and 4M hydrochloric acid in dioxane (10 mL). After 1 hour, the reaction mixture is evaporated in vacuo to give a residue. Triturate the residue with diethyl ether to give a solid. Collect the solid by filtration and dry in vacuo to give the title compound.

後処理

  1. customthe reaction mixture is evaporated in vacuo
  2. customto give a residue
  3. customTriturate the residue with diethyl ether
  4. customto give a solid
  5. customCollect the solid
  6. filtrationby filtration
  7. customdry in vacuo

出典と根拠

ORDレコード
ord-3745e05df16b4b459819b691d267c529
出典データセット
uspto-grants-1999_03
特許番号
US05877202

反応ノート

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