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HRID 1417804作成日：2026年10月27日

6-Chloro-1-(2-chloroethyl)isochroman → 1-[2-(6-Chloroisochroman-1-yl)ethyl]-4-(4-methoxyphenyl)piperazine dihydrochloride

https://huagongshe.com/reaction/1417804

反応式

関与物質

役割名称HCID仕込み量
反応物6-Chloro-1-(2-chloroethyl)isochromanHCID 23288787—
反応物1-[2-(Isochroman-1-yl)ethyl]-4-(2-methoxyphenyl)piperazine dihydrochloride monohydrateHCID 23288951—
生成物1-[2-(6-Chloroisochroman-1-yl)ethyl]-4-(4-methoxyphenyl)piperazine dihydrochlorideHCID 23288911—

反応手順

Following the general procedure of EXAMPLE 1 and making non-critical variations but using 6-chloro-1-(2-chloroethyl)isochroman (LXIV, 0.2315 g, 0.972 mmol) and 1-(4-methoxyphenyl)piperazine dihydrochloride (XI, 0.3772 g, 1.00 mmol), the title compound is obtained, mp 203.5°-208°; MS (m/z) 386; IR (mineral oil) 1512, 2388, 1485, 1261, 1118 and 1105 cm-1.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05877317
出典データセットuspto-grants-1999_03
ORD IDord-2dc94ca63ead4ca7a04c1e1221e90d09
出典メモuspto-grants-1999_03