2-t-Butyl-5-cyano-1-nitrobenzene → Benzonitrile, 3-amino-4-(1,1-dimethylethyl)-
反応式
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([C:11]#[N:12])=[CH:7][C:6]=1[N+:13]([O-])=O)([CH3:4])([CH3:3])[CH3:2]>CCCCCC.C(OCC)(=O)C>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([C:11]#[N:12])=[CH:7][C:6]=1[NH2:13])([CH3:4])([CH3:2])[CH3:3]参加物
3
実験手順
2-t-Butyl-5-cyano-1-nitrobenzene [prepared as described in step (i) above] was reduced in a similar manner to that described in Preparation 5 to give the title compound as crystals, melting at 94.5°-95° C. (from hexane-ethyl acetate).
後処理
- customdescribed in Preparation 5
出典と根拠
- ORDレコード
- ord-16a9739e907843e6b1d4f64b25e10041
- 出典データセット
- uspto-grants-1999_03
- 特許番号
- US05880147
反応ノート
読み込み中…