Pyruvic Acid → Creatine pyruvate monohydrate

HRID 1419204ノート

反応式

HRID 1419204 の反応式
O.[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:10])[NH2:9])[CH3:7])[OH:4].[C:11]([OH:16])(=[O:15])[C:12]([CH3:14])=[O:13].C(O)(C)C>O>[OH2:2].[C:11]([OH:16])(=[O:15])[C:12]([CH3:14])=[O:13].[O:2]=[C:3]([CH2:5][N:6]([C:8](=[NH:9])[NH2:10])[CH3:7])[OH:4]

参加物

5

反応物 3

HCID 1060Pyruvic AcidHCID 3776IsopropanolHCID 80116Creatine Monohydrate

生成物 1

HCID 9881182Creatine pyruvate monohydrate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

One mole of creatine monohydrate with a molecular weight of 149.15 g/mole is mixed with one mole of pyruvic acid having a molecular weight of 88.06 g/mole. To this mixture is added 20 gms of a 1:1 v/v mixture of isopropyl alcohol and water. The powder and liquid are stirred together while being held at or below 60° C. by a cooling bath at that temperature until the mixture solidifies. The resultant powder is dried to yield crystalline creatine pyruvate monohydrate. This product has a molecular weight of 237.21 and decomposes at 112°-114° C.

後処理

  1. additionTo this mixture is added
  2. custombelow 60° C.
  3. customThe resultant powder is dried

出典と根拠

ORDレコード
ord-1f6d8f297995436ba5cbf7b74b5cbc96
出典データセット
uspto-grants-1999_03
特許番号
US05886040

反応ノート

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