Hydrogen Peroxide → HCID 14455327、化合物
反応式
[C:1]([NH:6][C@@H:7]([C:10]([OH:12])=[O:11])[CH2:8][SH:9])(=[O:5])[CH:2]([CH3:4])[CH3:3].OO>CO>[CH3:3][CH:2]([CH3:4])[C:1]([NH:6][C@H:7]([CH2:8][S:9][S:9][CH2:8][C@@H:7]([NH:6][C:1](=[O:5])[CH:2]([CH3:3])[CH3:4])[C:10]([OH:12])=[O:11])[C:10]([OH:12])=[O:11])=[O:5]参加物
4
実験手順
N-isobutyryl-D-cysteine (1 g, 5.2 mmol) was dissolved in 10 ml of methanol. Hydrogen peroxide (30%, 0.3 ml, 2.6 mmol) was added and the reaction mixture was stirred at room temperature for 6 hours. After evaporation of the solvent under reduced pressure, a white crystallised oil was obtained. Recrystallisation from ethyl acetate furnished the title compound as a white solid which was dried in vacuo.
後処理
- customAfter evaporation of the solvent under reduced pressure
- customa white crystallised oil
- customwas obtained
- customRecrystallisation from ethyl acetate
出典と根拠
- ORDレコード
- ord-5ee1a527e2cd446a984390c5fca9ee42
- 出典データセット
- uspto-grants-1999_03
- 特許番号
- US05889050
反応ノート
読み込み中…