Isopentane → Isopentane alpha-cyclodextrin

HRID 1420468ノート

反応式

HRID 1420468 の反応式
[CH2:1]([OH:66])[C@H:2]1[O:7][C@@H:6]2[O:8][C@H:9]3[C@H:14]([OH:15])[C@@H:13]([OH:16])[C@@H:12]([O:17][C@H:18]4[C@H:23]([OH:24])[C@@H:22]([OH:25])[C@@H:21]([O:26][C@H:27]5[C@H:32]([OH:33])[C@@H:31]([OH:34])[C@@H:30]([O:35][C@H:36]6[C@H:41]([OH:42])[C@@H:40]([OH:43])[C@@H:39]([O:44][C@H:45]7[C@H:51]([OH:52])[C@@H:50]([OH:53])[C@@H:48]([O:49][C@H:3]1[C@H:4]([OH:65])[C@H:5]2[OH:64])[O:47][C@@H:46]7[CH2:54][OH:55])[O:38][C@@H:37]6[CH2:56][OH:57])[O:29][C@@H:28]5[CH2:58][OH:59])[O:20][C@@H:19]4[CH2:60][OH:61])[O:11][C@@H:10]3[CH2:62][OH:63].[CH3:67][CH2:68][CH:69]([CH3:71])[CH3:70]>>[CH3:67][CH2:68][CH:69]([CH3:71])[CH3:70].[CH2:56]([OH:57])[C@H:37]1[O:38][C@@H:39]2[O:44][C@H:45]3[C@H:51]([OH:52])[C@@H:50]([OH:53])[C@@H:48]([O:49][C@H:3]4[C@H:4]([OH:65])[C@@H:5]([OH:64])[C@@H:6]([O:8][C@H:9]5[C@H:14]([OH:15])[C@@H:13]([OH:16])[C@@H:12]([O:17][C@H:18]6[C@H:23]([OH:24])[C@@H:22]([OH:25])[C@@H:21]([O:26][C@H:27]7[C@H:32]([OH:33])[C@@H:31]([OH:34])[C@@H:30]([O:35][C@H:36]1[C@H:41]([OH:42])[C@H:40]2[OH:43])[O:29][C@@H:28]7[CH2:58][OH:59])[O:20][C@@H:19]6[CH2:60][OH:61])[O:11][C@@H:10]5[CH2:62][OH:63])[O:7][C@@H:2]4[CH2:1][OH:66])[O:47][C@@H:46]3[CH2:54][OH:55]

参加物

3

反応物 2

HCID 6556IsopentaneHCID 444913Alpha-Cyclodextrin

生成物 1

HCID 131721835Isopentane alpha-cyclodextrin

実験手順

20 ml of saturated α-cyclodextrin solution were mixed with 1 ml of isopentane and ultrasounded for 3 minutes in the ultrasonic bath. The resulting difficultly soluble complex was obtained through filtration and dried via calcium chloride.

後処理

  1. customThe resulting difficultly soluble complex was obtained through filtration
  2. dry with materialdried via calcium chloride

出典と根拠

ORDレコード
ord-654bed1612b04b9d917bf465415e688e
出典データセット
uspto-grants-2000_06
特許番号
US06071496

反応ノート

読み込み中…