Hydrochloric Acid → HCID 178479544、化合物
反応式
[C:1](#[N:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:9].C[OH:11]>>[ClH:9].[C:1](=[NH:8])([OH:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
4
実験手順
A solution of benzonitrile (20 g, 0.194 mol) in methanol (8 ml) was bubbled with gaseous HCl to saturation. The solution was allowed to stand overnight, and then a pale yellow solid was found. The solid was triturated with ether, filtered, washed with ether, and dried to yield beige solid product (32 g, 96%).
後処理
- customThe solid was triturated with ether
- filtrationfiltered
- washwashed with ether
- customdried
出典と根拠
- ORDレコード
- ord-505d79f556dc4fb48946a5bf8ccee1ed
- 出典データセット
- uspto-grants-2000_06
- 特許番号
- US06071913
反応ノート
読み込み中…