関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methane | HCID 297 | — |
| 反応物 | Hexanoic Acid | HCID 8892 | — |
| 反応物 | Ammonium Hydroxide | HCID 14923 | — |
| 生成物 | 3-Aminohexanoic acid | HCID 5275645 | — |
反応手順
A mixture of 2 hexanoic acid (7.0 g, 0.06 mole) and concentrated aqueous ammonium hydroxide (70 ml) is heated for 24 hours in an autoclave at 150° C. The cooled mixture is treated with carbon black and filtered. After evaporation of the solvent, the crude product is recrystallized from ethanol to give the title compound m.p. 203° C. (Compound 1.21, Table 1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06075051 |
|---|
| 出典データセット | uspto-grants-2000_06 |
|---|
| ORD ID | ord-3e066ec21d4e4a9d8864e13b0a802682 |
|---|
| 出典メモ | uspto-grants-2000_06 |
|---|
