Allyl chloride → HCID 11066618、化合物
反応式
[CH2:1](Cl)[CH:2]=[CH2:3].[CH2:5]([C:17]1[CH:22]=[CH:21][C:20]([OH:23])=[CH:19][CH:18]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH:14]([CH3:16])[CH3:15]>>[CH2:1]([O:23][C:20]1[CH:21]=[CH:22][C:17]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH:14]([CH3:16])[CH3:15])=[CH:18][CH:19]=1)[CH:2]=[CH2:3]参加物
3
反応条件
- 温度
- 63 °C
実験手順
Next, 363 grams (4.75M) of allyl chloride were added, and mixed with the fluid initial reaction product. The mixture was then heated to 63° C., and exothermed slowly to 73° C. A sample was taken at this point, then acidified and stripped under reduced pressure. TLC revealed the presence on the sample of a small amount of unreacted p-isododecylphenol.
後処理
- additionmixed with the fluid initial
- customreaction product
- customexothermed slowly to 73° C