関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1-Dodecanol | HCID 8193 | — |
| 反応物 | Ethyl mandelate | HCID 13050 | — |
| 生成物 | Lauryl mandelate | HCID 11587803 | 62.3% |
反応手順
A mixture of Novozym® 435 (2.21 g), molecular sieves (18.60 g), 1-dodecanol (3.76 g), and ethyl mandelate (3.61 g) in a 150 mL beaker was maintained at 60° C. in a convection oven for 28 hours. Upon work-up, 4.0 g of lauryl mandelate (56% yield) was obtained as a clear viscous liquid. The purity of the product was >95% as assessed by HPLC-DAD.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08936922B2 |
|---|
| 出典データセット | uspto-grants-2015_01 |
|---|
| ORD ID | ord-ffeba419d3fb46509f0159ed8518cca3 |
|---|
| 出典メモ | uspto-grants-2015_01 |
|---|
