化工社化工社 化学情報印刷レポート · 研究参考用
1-Phenylnaphthalene → Acryloyl-1-phenylnaphthalene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Phenylnaphthalene | HCID 11795 | — |
| 反応物 | Acryloyl chloride | HCID 13140 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Acryloyl-1-phenylnaphthalene | HCID 86673232 | 125.2% |
反応手順
1-phenylnaphthalene (204 mg), acryloyl chloride (200 mg), and aluminium chloride (290 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (323 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08937091B2 |
| 出典データセット | uspto-grants-2015_01 |
| ORD ID | ord-d3ef5e2ceed241289f186007c662443e |
| 出典メモ | uspto-grants-2015_01 |