Zirconium → gamma-Cyclodextrin Zirconium

HRID 1428697

反応式

HRID 1428697 の反応式
[Zr:1].[CH2:2]([OH:88])[C@H:3]1[O:8][C@@H:7]2[O:9][C@H:10]3[C@H:15]([OH:16])[C@@H:14]([OH:17])[C@@H:13]([O:18][C@H:19]4[C@H:24]([OH:25])[C@@H:23]([OH:26])[C@@H:22]([O:27][C@H:28]5[C@H:33]([OH:34])[C@@H:32]([OH:35])[CH:31]([O:36][CH:37]6[C@H:42]([OH:43])[C@@H:41]([OH:44])[CH:40]([CH:45]7[C@H:50]([OH:51])[C@@H:49]([OH:52])[CH:48]([O:53][C@H:54]8[C@H:59]([OH:60])[C@@H:58]([OH:61])[C@@H:57]([O:62][C@H:63]9[C@H:69]([OH:70])[C@@H:68]([OH:71])[C@@H:66]([O:67][C@H:4]1[C@H:5]([OH:87])[C@H:6]2[OH:86])[O:65][C@@H:64]9[CH2:72][OH:73])[O:56][C@@H:55]8[CH2:74][OH:75])[O:47][C@@H:46]7[CH2:76][OH:77])[O:39][C@@H:38]6[CH2:78][OH:79])[O:30][C@@H:29]5[CH2:80][OH:81])[O:21][C@@H:20]4[CH2:82][OH:83])[O:12][C@@H:11]3[CH2:84][OH:85]>>[CH2:2]([OH:88])[C@H:3]1[O:8][C@@H:7]2[O:9][C@H:10]3[C@H:15]([OH:16])[C@@H:14]([OH:17])[C@@H:13]([O:18][C@H:19]4[C@H:24]([OH:25])[C@@H:23]([OH:26])[C@@H:22]([O:27][C@H:28]5[C@H:33]([OH:34])[C@@H:32]([OH:35])[CH:31]([O:36][CH:37]6[C@H:42]([OH:43])[C@@H:41]([OH:44])[CH:40]([CH:45]7[C@H:50]([OH:51])[C@@H:49]([OH:52])[CH:48]([O:53][C@H:54]8[C@H:59]([OH:60])[C@@H:58]([OH:61])[C@@H:57]([O:62][C@H:63]9[C@H:69]([OH:70])[C@@H:68]([OH:71])[C@@H:66]([O:67][C@H:4]1[C@H:5]([OH:87])[C@H:6]2[OH:86])[O:65][C@@H:64]9[CH2:72][OH:73])[O:56][C@@H:55]8[CH2:74][OH:75])[O:47][C@@H:46]7[CH2:76][OH:77])[O:39][C@@H:38]6[CH2:78][OH:79])[O:30][C@@H:29]5[CH2:80][OH:81])[O:21][C@@H:20]4[CH2:82][OH:83])[O:12][C@@H:11]3[CH2:84][OH:85].[Zr:1]

参加物

3

反応物 2

HCID 23995Zirconium2 回HCID 44431027gamma-Cyclodextrine

生成物 1

HCID 131732362gamma-Cyclodextrin Zirconium

実験手順

23 g of a zirconium-based drier, Zirconium Hex-CEM® 12% solution (OM Group, Inc.) was added to the above-noted γ-cylodextrin solution. A white precipitate formed upon addition of the drier. The mixture was stirred for at least 16 hours. The precipitate was filtered off under reduced pressure. The precipitate was dried under normal conditions at ambient temperature. The FTIR spectrum of the resultant inclusion complex is provided in FIG. 1(e).

後処理

  1. customA white precipitate formed upon addition of the drier
  2. filtrationThe precipitate was filtered off under reduced pressure
  3. customThe precipitate was dried under normal conditions at ambient temperature
  4. customThe FTIR spectrum of the resultant inclusion complex is provided in FIG. 1(e)

出典と根拠

ORDレコード
ord-df05649b712f46fbbb7e52be5ff9f9aa
出典データセット
uspto-grants-2015_01
特許番号
US08937119B2

関連ノート

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