化工社化工社 化学情報印刷レポート · 研究参考用
5,6,7,8-Tetrahydro-2-naphthylamine → 1-(1-oxo-1,2,7,8,9,10-hexahydro-benzo[f]quinazolin-3-yl)-1H-pyrazole-4-carboxylic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5,6,7,8-Tetrahydro-2-naphthylamine | HCID 75193 | — |
| 反応物 | 1-(4-oxo-3,4,6,7,8,9-hexahydro-benzo[g]quinazolin-2-yl)-1H-pyrazole-4-carboxylic acid ethyl ester | HCID 136337181 | — |
| 生成物 | 1-(1-oxo-1,2,7,8,9,10-hexahydro-benzo[f]quinazolin-3-yl)-1H-pyrazole-4-carboxylic acid ethyl ester | HCID 136337182 | — |
反応手順
The titled compound was prepared in a manner analogous to Example 131, steps A-B, using 5,6,7,8-tetrahydro-naphthalen-2-ylamine in step A. Step B yielded a 2:1 mixture of 1-(4-oxo-3,4,6,7,8,9-hexahydro-benzo[g]quinazolin-2-yl)-1H-pyrazole-4-carboxylic acid ethyl ester and the titled compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08937078B2 |
| 出典データセット | uspto-grants-2015_01 |
| ORD ID | ord-06b0dac4f44646938b8643ded06d85c2 |
| 出典メモ | uspto-grants-2015_01 |