2-Acetylthiophene → 2-Acetylthiophene 4-fluorophenylhydrazone

反応式

Cl.[F:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][NH2:10])=[CH:5][CH:4]=1.[C:11]([C:14]1[S:15][CH:16]=[CH:17][CH:18]=1)(=O)[CH3:12]>>[F:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][N:10]=[C:11]([C:14]2[S:15][CH:16]=[CH:17][CH:18]=2)[CH3:12])=[CH:5][CH:4]=1

参加物

反応物 2

HCID 69202-Acetylthiophene

HCID 699814-Fluorophenylhydrazine hydrochloride

生成物 1

HCID 849242442-Acetylthiophene 4-fluorophenylhydrazone

実験手順

This compound is prepared from commercial 4-fluorophenylhydrazine hydrochloride (Aldrich) and from commercial 2-acetylthiophene (Aldrich), according to the procedure 1.

出典と根拠

ORDレコード: ord-a1000e40f2db412d9d636d6f712f48b1
出典データセット: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05726063

反応ノート

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