Phenylhydrazine hydrochloride → 2-Acetylselenophene phenylhydrazone

反応式

Cl.[C:2]1([NH:8][NH2:9])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10]([C:13]1[Se:14][CH:15]=[CH:16][CH:17]=1)(=O)[CH3:11]>>[C:2]1([NH:8][N:9]=[C:10]([C:13]2[Se:14][CH:15]=[CH:16][CH:17]=2)[CH3:11])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

参加物

反応物 2

HCID 60962Phenylhydrazine hydrochloride

HCID 139932Ethanone, 1-selenophene-2-yl-

生成物 1

HCID 867521872-Acetylselenophene phenylhydrazone

実験手順

This compound is prepared from commercial phenylhydrazine hydrochloride (Aldrich) and 2-acetylselenophene, which is itself obtained according to the procedure described by S. Umezawa (reference 18).

後処理

customobtained

出典と根拠

ORDレコード: ord-b1c4c35e4d754049b51187394fb98649
出典データセット: uspto-grants-1998_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05726063

反応ノート

読み込み中…