化工社化工社 化学情報印刷レポート · 研究参考用
6-Aminohexanoic Acid → HCID 178512818、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Aminohexanoic Acid | HCID 564 | — |
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Methanesulfonic acid, aminoimino- | HCID 9877361 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178512818 | HCID 178512818 | — |
反応手順
6.5 g (50 mmol) 6-aminohexanoic acid and 6.9 g (50 mmol) sodium carbonate were dissolved in 50 mL water. 6.2 g (50 mmol) amino-iminomethane sulphonic acid was added under stirring to the solution. After 20 hours, the product was filtered and washed with acetic acid, methanol and then ether. Yield: 6.6 g (76%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07732378B2 |
| 出典データセット | uspto-grants-2010_06 |
| ORD ID | ord-5a319964270d42289d6889c6bc678cfb |
| 出典メモ | uspto-grants-2010_06 |