6-Aminohexanoic Acid → HCID 178512818、化合物

HRID 14366

反応式

HRID 14366 の反応式
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].C(=O)([O-])[O-].[Na+].[Na+].[NH2:16][C:17](=[NH:22])S(O)(=O)=O>O>[NH:1]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8])[C:17]([NH2:22])=[NH:16]

参加物

5

反応物 3

HCID 5646-Aminohexanoic AcidHCID 10340Sodium CarbonateHCID 9877361Methanesulfonic acid, aminoimino-

生成物 1

HCID 178512818HCID 178512818、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

6.5 g (50 mmol) 6-aminohexanoic acid and 6.9 g (50 mmol) sodium carbonate were dissolved in 50 mL water. 6.2 g (50 mmol) amino-iminomethane sulphonic acid was added under stirring to the solution. After 20 hours, the product was filtered and washed with acetic acid, methanol and then ether. Yield: 6.6 g (76%).

後処理

  1. filtrationthe product was filtered
  2. washwashed with acetic acid, methanol

出典と根拠

ORDレコード
ord-5a319964270d42289d6889c6bc678cfb
出典データセット
uspto-grants-2010_06
特許番号
US07732378B2

関連ノート

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