Methanesulfonyl chloride → HCID 86606810、化合物
反応式
Cl.[F:2][C:3]([F:29])([F:28])[C:4]1[CH:5]=[C:6]([CH:21]=[C:22]([C:24]([F:27])([F:26])[F:25])[CH:23]=1)[CH2:7][O:8][C@H:9]1[CH2:14][CH2:13][NH:12][CH2:11][C@H:10]1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[CH3:30][S:31](Cl)(=[O:33])=[O:32]>>[F:29][C:3]([F:2])([F:28])[C:4]1[CH:5]=[C:6]([CH:21]=[C:22]([C:24]([F:27])([F:25])[F:26])[CH:23]=1)[CH2:7][O:8][C@H:9]1[CH2:14][CH2:13][N:12]([S:31]([CH3:30])(=[O:33])=[O:32])[CH2:11][C@H:10]1[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1参加物
3
実験手順
The compound (0.15 g) obtained in Example 1 and methylsulfonyl chloride (0.040 ml) were reacted and treated in the same manner as in the method described in Example 2 to obtain the title compound as colorless oil (0.093 g, 57%).
後処理
- additiontreated in the same manner as in the method
出典と根拠
- ORDレコード
- ord-afc3690ddad54548a2d2dc8d77326275