Ethyl 2-isocyanatobenzoate → HCID 86606826、化合物
反応式
[CH2:1]([C@H:8]1[C@@H:13]([O:14][CH2:15][C:16]2[CH:21]=[C:20]([C:22]([F:25])([F:24])[F:23])[CH:19]=[C:18]([C:26]([F:29])([F:28])[F:27])[CH:17]=2)[CH2:12][CH2:11][NH:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N:30]([C:33]1[CH:43]=[CH:42][CH:41]=[CH:40][C:34]=1[C:35]([O:37][CH2:38][CH3:39])=[O:36])=[C:31]=[O:32]>CCN(CC)CC>[CH2:1]([CH:8]1[CH:13]([O:14][CH2:15][C:16]2[CH:17]=[C:18]([C:26]([F:29])([F:27])[F:28])[CH:19]=[C:20]([C:22]([F:23])([F:24])[F:25])[CH:21]=2)[CH2:12][CH2:11][N:10]([C:31]([NH:30][C:33]2[CH:43]=[CH:42][CH:41]=[CH:40][C:34]=2[C:35]([O:37][CH2:38][CH3:39])=[O:36])=[O:32])[CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
4
実験手順
The compound (0.15 g) obtained in Example 404 and ethyl 2-isocyanatobenzoate (0.076 mg) were reacted and treated in the same manner as in the method described in Example 6 excluding Et3N to obtain the title compound as pale yellow oil (0.139 g, 64%).