Triethylenetetramine → HCID 20327359、化合物

HRID 1439310ノート

反応式

HRID 1439310 の反応式
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2CC(=O)CC1CC2CC1CC2.[CH2:19]([CH2:22][NH:23][CH2:24][CH2:25][CH2:26][NH2:27])[CH2:20][NH2:21].[ClH:28].Cl.Cl.Cl.[CH:32]12[CH2:38][CH:35]([CH2:36][CH2:37]1)[CH2:34][CH:33]2[CH2:39][CH:40](NCCNCCNCCN)[CH2:41][CH:42]1CC2C[CH:43]1CC2.NCCNCCNCCN.Cl.Cl.Cl.C12CC(CC1)CC2CCCC(NCCCNCCCN)CCCC1CC2CC1CC2.CCCC(=O)CCC.Cl.Cl.Cl.C12CC(CC1)CC2C(CC(NCCCNCCCN)CC(C1CC2CC1CC2)C)C.C12CC(CC1)CC2C(CC(=O)CC(C1CC2CC1CC2)C)C>>[ClH:28].[ClH:28].[ClH:28].[CH:32]12[CH2:38][CH:35]([CH2:36][CH2:37]1)[CH2:34][CH:33]2[CH2:39][CH2:40][CH:41]([NH:21][CH2:20][CH2:19][CH2:22][NH:23][CH2:24][CH2:25][CH2:26][NH2:27])[CH2:42][CH2:43][CH:2]1[CH2:3][CH:4]2[CH2:7][CH:1]1[CH2:6][CH2:5]2

参加物

9

反応物 8

HCID 5565TriethylenetetramineHCID 5942Bis(3-aminopropyl)amine3 回HCID 312464-HeptanoneHCID 19850365HCID 19850365、化合物2 回HCID 203273291-[2,6-Di(2-norbornyl)-4-heptyl]-1,5,9-triazanonane trihydrochlorideHCID 20327336HCID 20327336、化合物HCID 203273501-[1,7-Di-(2-norbornyl)-4-heptyl]-1,5,9-triazanonane trihydrochlorideHCID 213906161-[1,3-Di-2-norbornyl-2-propyl]-1,4,7,10-tetraazadecane tetrahydrochloride

生成物 1

HCID 20327359HCID 20327359、化合物

実験手順

Also prepared by this method in an analogous manner regarding molar quantities and reaction conditions are 1[1,3-(2-norbornyl)-2-propyl] -1,5,9-triazanonane trihydrochloride from 1,3-di-(2-norbornyl)-2-propanone and 3,3'-iminobispropylamine; 1-[1,3-di-2-norbornyl-2-propyl] -1,4,7,10-tetraazadecane tetrahydrochloride from 1,3-di-(2-norbornyl)-2-propanone and triethylenetetramine; 1-[1,7-di-(2-norbornyl)-4-heptyl]-1,5,9-triazanonane trihydrochloride from 1,7-di-2-norbornyl)-4-heptanone and 3,3'-iminobispropylamine and 1-[2,6-di-(2-norbornyl)-4-heptyl] -1,5,9-triazanonane trihydrochloride from 2,6-di-(2-norbornyl)-4-heptanone and 3,3'-iminobispropylamine.

後処理

  1. customAlso prepared by this method in an analogous manner
  2. customquantities and reaction conditions

出典と根拠

ORDレコード
ord-c98ee522aba549119f9240d5180ba959
出典データセット
uspto-grants-1977_11
特許番号
US04058625

反応ノート

読み込み中…