Benzoyl chloride, 3,4,5-trimethoxy- → 1-Amino-3-[(1,1-dimethylethyl)(phenylmethyl)amino]propan-2-OL

HRID 1439427

反応式

HRID 1439427 の反応式
Cl.COC1C=C(C=C(OC)C=1OC)C([NH:9][CH2:10][CH:11]([OH:25])[CH2:12][N:13]([C:21]([CH3:24])([CH3:23])[CH3:22])[CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=O.COC1C=C(C=C(OC)C=1OC)C(Cl)=O>>[NH2:9][CH2:10][CH:11]([OH:25])[CH2:12][N:13]([C:21]([CH3:23])([CH3:22])[CH3:24])[CH2:14][C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

参加物

3

反応物 2

HCID 78282Benzoyl chloride, 3,4,5-trimethoxy-HCID 213976361-(3,4,5-trimethoxy benzamido)-3-(N-benzyl tert-butylamino)-2-propanol hydrochloride

生成物 1

HCID 30165241-Amino-3-[(1,1-dimethylethyl)(phenylmethyl)amino]propan-2-OL収率 78%

実験手順

1-(3,4,5-trimethoxy benzamido)-3-(N-benzyl tert-butylamino)-2-propanol hydrochloride, starting from 7.8 g (0.034 mole) of 3,4,5-trimethoxy benzoyl chloride and 8 g (0.034 mole) of 1-amino-3-(N-benzyl tert-butylamino)-2-propanol (yield 78 %).

出典と根拠

ORDレコード
ord-677ff1ef6ddc4c7cbc917112ba88a232
出典データセット
uspto-grants-1977_11
特許番号
US04059621

関連ノート

読み込み中…