Anthranilamide → HCID 11345158、化合物

HRID 1439611ノート

反応式

HRID 1439611 の反応式
[NH2:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[CH2:11](Cl)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>O>[CH2:11]([NH:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

参加物

4

反応物 2

HCID 6942AnthranilamideHCID 7503Benzyl Chloride

生成物 1

HCID 11345158HCID 11345158、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

To a hot solution of 20 g Na OHin 1250 ml water was added 68 g 2-aminobenzamide followed by 58 ml benzyl chloride. The mixture was refluxed 20 minutes, cooled and the solid filtered and washed with water. The product was recrystallized from 95% alcohol to give 62 g, m.169-73°.

後処理

  1. temperatureThe mixture was refluxed 20 minutes
  2. temperaturecooled
  3. filtrationthe solid filtered
  4. washwashed with water
  5. customThe product was recrystallized from 95% alcohol
  6. customto give 62 g, m
  7. custom169-73°

出典と根拠

ORDレコード
ord-3939ffe401a54a14a08aa648fbedeb04
出典データセット
uspto-grants-1977_11
特許番号
US04060526

反応ノート

読み込み中…