関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Octadecyl isocyanate | HCID 66988 | — |
| 反応物 | 1,1,2,2-Tetrahydroperfluoro-1-decanol | HCID 69619 | — |
| 生成物 | HCID 131719350 | HCID 131719350 | — |
反応手順
Octadecyl isocyanate (29.5 g, 0.1 moles) and C8F17CH2CH2OH (46.4 g, 0.1 moles) were mixed under nitrogen and heated with stirring to 90° C. for 8 hours. An infrared spectrum showed no -NCO absorption, indicating completion of the reaction. The product is a white wax melting at 72-75° C. NMR showed proton resonances at 4.7 ppm (1 proton NH), 4.4 ppm (2 proton CH2OCO-), 3.2 ppm (2 protons CH2CH2NH), 2.5 ppm (2 protons C8F17CH2), 1.3 ppm (32 protons CH3(CH2)16) and 0.8 ppm (3 protons CH3 (CH2)16).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05502225 |
|---|
| 出典データセット | uspto-grants-1996_03 |
|---|
| ORD ID | ord-47acc5b0da33457db4093a1ca3fd21a6 |
|---|
| 出典メモ | uspto-grants-1996_03 |
|---|
